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A novel gold( i )-catalyzed chemo- and site-selective cascade C–H functionalization/dearomatization of naphthols or phenols with  o -alkynylaryl-α-diazoesters has been developed.

chemical communications

Gold-catalyzed intermolecular [4+1] spiroannulation <i>via</i> site-selective aromatic C(sp<sup>2</sup>)–H functionalization and dearomatization of phenol derivatives

Gold-catalyzed intermolecular [4+1] spiroannulation via site-selective aromatic C(sp2)–H functionalization and dearomatization of phenol derivatives

Gold-catalyzed intermolecular [4+1] spiroannulation via site-selective aromatic C(sp²)–H functionalization and dearomatization of phenol derivatives