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A highly efficient method for controllable double CF 2 -insertion into pentafluorophenylcopper species using TMSCF 3 as difluoromethylene source has been developed. The newly generated fluoroalkylcopper(i) species, C 6 F 5 CF 2 CF 2 Cu, shows good reactivity towards a myriad of structurally diverse aryl, heteroaryl and alkenyl iodides. This protocol is easy to handle, ready to scale up and applicable for the synthesis of relative complex molecules, thus providing a convenient method for facile access to tetrafluoroethylene-bridged structures.

chemical science

Controllable double CF2-insertion into sp2 C–Cu bond using TMSCF3: a facile access to tetrafluoroethylene-bridged structures