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Rhodium(ii)-catalyzed unusual branch-selective ortho -C-H alkylation of aryl sulfonamides with vinylsilanes was achieved using an 8-aminoquinoline directing group. Notably, the para -substituted aryl sulfonamides gave mono-(branched)alkylated products exclusively without the formation of any double C-H alkylated byproducts. The results of deuterium labeling experiments suggest that both hydrometalation and carbometalation pathways are involved in this conversion.

Rh(ii)-catalyzed branch-selective C–H alkylation of aryl sulfonamides with vinylsilanes