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Treatment of multi-walled carbon nanotubes (MWCNTs) with a boiling nitrating mixture proceeds  via  two interrelated phenomena,  i.e.  periodic-like carboxylation and layer-by-layer desheathing, and overall, it can be controlled by kinetics of the process.

rsc advances

Selective carboxylation <i>versus</i> layer-by-layer unsheathing of multi-walled carbon nanotubes: new insights from the reaction with boiling nitrating mixture

Selective carboxylation versus layer-by-layer unsheathing of multi-walled carbon nanotubes: new insights from the reaction with boiling nitrating mixture