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The current work shows an iron-catalyzed 2-aza-Cope rearrangement in dimethyl carbonate for the synthesis of a wide variety of α-substituted homoallylamines from readily accessible starting materials with diverse functional groups.

Lewis acidic FeCl3 promoted 2-aza-Cope rearrangement to afford α-substituted homoallylamines in dimethyl carbonate

Lewis acidic FeCl₃ promoted 2-aza-Cope rearrangement to afford α-substituted homoallylamines in dimethyl carbonate