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An efficient photocatalyst of boron-doped titanium dioxide/titanium nanotube array-supported platinum particles (Pt-B/TiO 2 /Ti NTs) was fabricated for photocatalytic water splitting for hydrogen production through a two-step route. First, B/TiO 2 /Ti NTs were prepared by anodic oxidation using hydrofluoric acid as electrolyte and boric acid as a B source. Then, Pt particles were deposited on the surface of B/TiO 2 /Ti NTs by photo-assisted impregnation reduction. The structure and properties of Pt-B/TiO 2 /Ti NTs were characterized by various physical measurements which showed the successful fabrication of Pt-B/TiO 2 /Ti NTs. The Pt-B/TiO 2 /Ti NTs, with a B-doping content of 15 mmol L -1 , showed the highest photocatalytic activity and exhibited a photocatalytic hydrogen-production rate of 384.9 μmol g -1 h -1 , which was 9.2-fold higher than that of unmodified TiO 2 /Ti NTs (41.7 μmol g -1 h -1 ). This excellent photocatalytic performance was ascribed mainly to the synergistic effect of Pt and B, which could enhance the photocatalytic activity of TiO 2 /Ti NTs.

rsc advances

Deposition of platinum on boron-doped TiO<sub>2</sub>/Ti nanotube arrays as an efficient and stable photocatalyst for hydrogen generation from water splitting

Deposition of platinum on boron-doped TiO2/Ti nanotube arrays as an efficient and stable photocatalyst for hydrogen generation from water splitting

Deposition of platinum on boron-doped TiO₂/Ti nanotube arrays as an efficient and stable photocatalyst for hydrogen generation from water splitting