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A novel oxidation system in which magnesium nitrate [Mg(NO 3 ) 2 ] is used as an oxidant in the presence of diphe-nylphosphine oxide [HP(O)Ph 2 ] permits the C(sp 3 )-H hydroxylation of fluorenes, oxindoles, and benzofuranones. This method features high efficiency, good functional group tolerance, and operational simplicity. The synthetic utility is highlighted by further transformations to valuable organic materials.

organic chemistry frontiers

C(sp3)–H hydroxylation of fluorenes, oxindoles and benzofuranones with a Mg(NO3)2–HP(O)Ph2 oxidation system