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The characterization of a decanuclear Fe III cluster with α-methyl-2-pyridinemethanolate, generated by the hydrolysis of Schiff bases, inspired us to carry out an initial exploration of the direct syntheses of medium nuclearity Fe III clusters starting from aldehydes in methanolic medium. The new complexes exhibit an unprecedented {Fe 10 (μ 3 -O) 8 } cluster core.

Decanuclear FeIII clusters with hemiacetal ligands: a new {M10(μ3-O)8} cluster core

Decanuclear Fe^III clusters with hemiacetal ligands: a new {M₁₀(μ₃-O)₈} cluster core