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Geminal 18 F-oxyfluorination of diazoketones was performed in the presence of rhodium mediators. The reactions were performed using a hypervalent iodine-based [ 18 F]fluoro-benziodoxole reagent. By this methodology various α-[ 18 F]fluoro ethers were obtained in high radiochemical yield (up to 98%) and molar activity (216 GBq μmol -1 ).

Rhodium-mediated 18F-oxyfluorination of diazoketones using a fluorine-18-containing hypervalent iodine reagent

Rhodium-mediated ¹⁸F-oxyfluorination of diazoketones using a fluorine-18-containing hypervalent iodine reagent