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We realized that tailoring the pore size/geometry and chemistry, by virtue of alkynyl or naphthalene replacing phenyl within a series of isomorphic MOFs, can optimize methane storage working capacities, affording an exceptionally high working capacity of 203 cm 3 (STP) cm -3 at 298 K and 5-80 bar.

Tailoring the pore geometry and chemistry in microporous metal–organic frameworks for high methane storage working capacity