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Cation order, with a local structure related to γ-LiFeO 2 , is observed in the nominally cation-disordered Li-excess rocksalt Li 1.25 Nb 0.25 Mn 0.5 O 2 via X-ray diffraction, neutron pair distribution function analysis, magnetic susceptibility and NMR spectroscopy. The correlation length of ordering depends on synthesis conditions and has implications for the electrochemistry of these phases.

Short-range ordering in a battery electrode, the ‘cation-disordered’ rocksalt Li1.25Nb0.25Mn0.5O2

Short-range ordering in a battery electrode, the ‘cation-disordered’ rocksalt Li_1.25Nb_0.25Mn_0.5O₂