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Covalent post-synthetic functionalisation of layered metal-organic frameworks is demonstrated as a new approach to forming ultrathin nanosheets for use in catalysis. An aminoterephthalate framework was partially functionalised with sulfonate chains and exfoliated to form predominantly monolayer nanosheets able to catalyse a two-step acid-base reaction in one pot.

Tandem catalysis by ultrathin metal–organic nanosheets formed through post-synthetic functionalisation of a layered framework