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Insertion of a P- anion into a P-P bond yielding the first carborane-substituted 1,2,3-triphospholanide 1 was achieved by treating a carborane-substitued 1,2-diphosphetane with sodium phosphaethynolate. The triphospholanide 1 can serve as a versatile nucleophilic building block for unprecedent functionalised triphospholanes and carborane-substituted polyphosphanes.

Molecular doping: accessing the first carborane-substituted 1,2,3-triphospholanide via insertion of P− into a P−P bond

Molecular doping: accessing the first carborane-substituted 1,2,3-triphospholanide via insertion of P⁻ into a P−P bond