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An efficient transition-metal free C–C bond cleavage/borylation of cycloketone oxime esters has been described. In this reaction, the B 2 (OH) 4  reagent not only served as the boron source but also acted as an electron donor source through formation of a complex with a DMAc-like Lewis base.

Transition-metal free C–C bond cleavage/borylation of cycloketone oxime esters