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Both CNT and NCNT catalysts presented marked deactivation after activating PMS. Moreover, the initial activities of deactivated CNT and NCNT were restored by thermal treatment at different temperatures (T-350, T-550 and T-750) and chemical reduction (R–NaBH 4 ).

rsc advances

Deactivation and regeneration of carbon nanotubes and nitrogen-doped carbon nanotubes in catalytic peroxymonosulfate activation for phenol degradation: variation of surface functionalities