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A simple, efficient, and mild method for defluorination and functionalization of 3,3,3-trifluoro carbonyl compounds has been developed. In the present method, Cs 2 CO 3 can easily convert α-trifluoromethyl esters, amides, and ketones into β,β- S -, O - and/or N -substituted α,β-unsaturated carbonyl compounds in the presence of N -, O -, and S -nucleophiles with moderate to excellent yields, and furthermore, this transformation with α-trifluoromethyl ester and a series of 2-aminophenols can result in benzooxazoles in good yields.

rsc advances

Cs2CO3-promoted defluorination and functionalization of α-CF3carbonyl compounds in the presence ofN-,O-, and/orS-nucleophiles