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Thionocarbonate (–O–CS–O–) and xanthate (–S–CS–O–) cyclic monomers were synthesised by cyclothiocarbonation of 2-deoxy-D-ribose- and D-xylose-derived diols with carbon disulfide, then polymerised using organocatalytic ring-opening methods. Regular polymer linkages were obtained, with the sugar backbone influencing the regioselectivity of monomer opening. Thermal analysis revealed lower glass transition temperatures compared to carbonate analogues and a low onset of thermal degradation.

polymer chemistry

Polymers from sugars and CS<sub>2</sub>: synthesis and ring-opening polymerisation of sulfur-containing monomers derived from 2-deoxy-<scp>d</scp>-ribose and <scp>d</scp>-xylose

Polymers from sugars and CS2: synthesis and ring-opening polymerisation of sulfur-containing monomers derived from 2-deoxy-d-ribose and d-xylose

Polymers from sugars and CS₂: synthesis and ring-opening polymerisation of sulfur-containing monomers derived from 2-deoxy-d-ribose and d-xylose