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The coordination chemistry of Co(ii) with the chelating dicarboxylate ligand esp (esp = α,α,α',α'-tetramethyl-1,3-benzenedipropionate) is explored. We report here the bimetallic paddlewheel-type dimer, Co2(esp)2(EtOH)2 (1), and a bowl-shaped, heptanuclear coordination cluster, Co7(OH)4(Hesp)2(esp)4(MeCN)2·4MeCN (2). Crystal structures of both complexes are reported as well as their magnetic properties, which indicate antiferromagnetic interactions among the Co(ii) ions.

Cobalt complexes of the chelating dicarboxylate ligand “esp”: a paddlewheel-type dimer and a heptanuclear coordination cluster