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Fast (&gt;100 kHz) magic angle spinning solid-state NMR allows combining high-sensitive proton detection with the absence of an intrinsic molecular weight limit. Using this technique we observe for the first time narrow 1 H RNA resonances and assign nucleotide spin systems with only 200 μg of uniformly 13 C, 15 N-labelled RNA.

Rapid access to RNA resonances by proton-detected solid-state NMR at >100 kHz MAS