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Hybrid core–shell Au/CeO2 nanoparticles (NPs) dispersed in UiO-66 shaped into microspherical beads are created using the spray-drying continuous-flow method. The combined catalytic properties of nanocrystalline CeO2 and Au in a single particle and the support and protective function of porous UiO-66 beads make the resulting composites show good performances as catalysts for CO oxidation (T50 = 72 °C; T100 = 100 °C) and recyclability.

Core–shell Au/CeO2 nanoparticles supported in UiO-66 beads exhibiting full CO conversion at 100 °C

Core–shell Au/CeO₂ nanoparticles supported in UiO-66 beads exhibiting full CO conversion at 100 °C