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Photoredox catalysis has been developed to achieve oxidative C-H chlorination of aromatic compounds using NaCl as the chlorine source and Na 2 S 2 O 8 as the oxidant. The reactions occur at room temperature and exhibit exclusive selectivity for C(sp 2 )-H bonds over C(sp 3 )-H bonds. The method has been used for the chlorination of a diverse set of substrates, including the expedited synthesis of key intermediates to bioactive compounds and a drug.

Room temperature C(sp2)–H oxidative chlorination via photoredox catalysis

Room temperature C(sp²)–H oxidative chlorination via photoredox catalysis