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The very rare occurrence of a gas-solid chemical reaction has been found to take place on a molecule within a compact non-porous crystal without destroying its long-range structural order and retaining similar crystal structures when yellow crystals of FeII4( mbm ) 4 Cl 4 (MeOH) 4 were exposed to air to give black [FeIII4( mbm ) 4 Cl 4 (OH) 4 ]·2H 2 O. The latter cannot be synthesised directly. The original cluster underwent an exchange of methanol to hydroxide, an oxidation of Fe(ii) to Fe(iii), a change in stereochemistry and hydration while the packing and space-group remained unaltered.

Chemical reaction within a compact non-porous crystal containing molecular clusters without the loss of crystallinity