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Copper-catalyzed selective coupling of C(sp 3 )-H bonds with C(sp 2 )-H bonds has been developed. An aniline module was used as a directing group to generate an aminyl radical, which selectively cleaves the secondary and tertiary C(sp 3 )-H bonds via a 1,5-HAT process to forge six-membered carbocyclic rings.

Copper-catalyzed oxidative C(sp3)–H/C(sp2)–H cross-coupling en route to carbocyclic rings

Copper-catalyzed oxidative C(sp³)–H/C(sp²)–H cross-coupling en route to carbocyclic rings