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In this work, nitrogen-doped honeycomb-like carbon framework (CNFs) is synthesized by a low-cost and scalable method. Ni nanoparticles are then supported on CNFs (CNFs–Ni) as a catalyst for methanol oxidation. In addition to the enhanced mass activity, both the onset and oxidation peak potentials of CNFs–Ni for methanol oxidation shift negatively in comparison to its non-doped counterpart, CFs–Ni. We propose that the small particle size, uniform dispersion, and electronic effect arising from the electron interactions between CNFs and Ni contribute to the improved electrocatalytic performance.

Nickel nanoparticles supported on nitrogen-doped honeycomb-like carbon frameworks for effective methanol oxidation