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A metal-free oxidation system employing tert-butyl hydroperoxide (TBHP) has been developed for selective oxidation of structurally diverse benzylic sp3 C–H bonds. This low-cost methodology allows for rapid generation of synthetically and biologically valued arylketones in good to excellent yields from readily available alkylarenes and diarylmethanes.

TBHP-promoted direct oxidation reaction of benzylic Csp3–H bonds to ketones

TBHP-promoted direct oxidation reaction of benzylic C_sp3–H bonds to ketones