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A chip-based platform for laser desorption/ionization mass spectrometry (LDI-MS) analysis of small molecules was developed by utilizing layer-by-layer (LBL) assembly of MoS 2 nanoflakes and polyallylamine on an arbitrary substrate. The LDI-MS efficiency of small molecules on MoS 2 films increased as a function of LBL assembly cycles until reaching a saturation point. The optimized MoS 2 nanoflake film exhibits high LDI-MS efficiency, salt tolerance, reusability and uniform ionic signal distribution, and its performance was further enhanced by surface modification with perfluoroalkanes mimicking a clathrate nanostructure.

nanoscale

A layer-by-layer assembled MoS<sub>2</sub> thin film as an efficient platform for laser desorption/ionization mass spectrometry analysis of small molecules

A layer-by-layer assembled MoS2 thin film as an efficient platform for laser desorption/ionization mass spectrometry analysis of small molecules

A layer-by-layer assembled MoS₂ thin film as an efficient platform for laser desorption/ionization mass spectrometry analysis of small molecules