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Herein we report the preparation of ammonium [ 11 C]thiocyanate via the reaction of [ 11 C]CS 2 with ammonia. The [ 11 C]SCN - ion is demonstrated as a potent nucleophile that can be used to readily generate a range of 11 C-labelled thiocyanate molecules in high conversions. Furthermore, novel 11 C-labelled thiazolone molecules can be easily prepared from the intermediate α-thiocyanatophenones via an acid mediated cyclisation reaction.

Ammonium [11C]thiocyanate: revised preparation and reactivity studies of a versatile nucleophile for carbon-11 radiolabelling

Ammonium [¹¹C]thiocyanate: revised preparation and reactivity studies of a versatile nucleophile for carbon-11 radiolabelling