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The solvothermal reaction between Cr(acac) 3 , MCl 2 ·6H 2 O (M = Ni, Co) and 2-hydroxy-4-methyl-6-phenyl-pyridine-3-amidoxime (H 2 L), under basic conditions, led to the synthesis of the heterometallic heptanuclear clusters [MCr(HL zw ) 6 (HL) 6 ]·3Cl (M = Ni, 1; Co, 2), with the nickel analogue displaying an S = 9/2 spin ground-state.

Constructing CrIII-centered heterometallic complexes: [NiII6CrIII] and [CoII6CrIII] wheels

Constructing Cr^III-centered heterometallic complexes: [NiII6Cr^III] and [CoII6Cr^III] wheels