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This communication presents the first synthesis of nanoconfined Lithium closo-borate, Li 2 B 12 H 12 , using nanoporous SiO 2 as scaffold. The yield of Li 2 B 12 H 12 is up to 94 mol%. The as-synthesized nanoconfined Li 2 B 12 H 12 exhibits a structural transition around 380 °C and conversion to H-deficiency Li 2 B 12 H 12-x at 580 °C.

Synthesis, stability and Li-ion mobility of nanoconfined Li2B12H12

Synthesis, stability and Li-ion mobility of nanoconfined Li₂B₁₂H₁₂