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A series of Ru II complexes stabilized with the pentapyridyl ligand Py 5 Me 2 (Py 5 Me 2 = 2,6-bis(1,1-bis(2-pyridyl)ethyl)pyridine) and with an axial X ligand (X = Cl - , H 2 O, N 3  - , MeCN) were prepared and characterized in the solid state and in non-aqueous solution. The cyclic voltammograms of these complexes in MeCN reflect a reversible substitution of the axial X ligand with MeCN. Irreversible ligand substitution of [(Py 5 Me 2 )RuN 3 ] + is also observed in propylene carbonate, but only at oxidizing potentials that decompose the azide ligand. The monometallic chloride and azide species are compared with analogous Ru 2 metal-metal bonded complexes, which have been reported to undergo irreversible chloride dissociation upon reduction.

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Synthesis, characterization and solution behavior of a systematic series of pentapyridyl-supported Ru<sup>II</sup> complexes: comparison to bimetallic analogs

Synthesis, characterization and solution behavior of a systematic series of pentapyridyl-supported RuII complexes: comparison to bimetallic analogs

Synthesis, characterization and solution behavior of a systematic series of pentapyridyl-supported Ru^II complexes: comparison to bimetallic analogs