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The effect of oxidative treatments on the depostion of cobalt nanocrystals (Co-NC) onto a support and subsequent ligand removal was investigated. Deposition of ε-cobalt NC led to extensive clustering of NC and low Fischer-Tropsch synthesis activity. Low-temperature oxidation of ε-cobalt NC resulted in a very uniform CoO-NC distribution and high activity whereas high-temperature oxidation to Co 3 O 4 led to less uniform NC distributions and lower activity.

Assembly and activation of supported cobalt nanocrystal catalysts for the Fischer–Tropsch synthesis