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We report a {Cu 16 } embedded within a {W 44 } cluster containing four cubane-like [Cu 4 O 4 ] units within an isopolyoxotungstate (isoPOT) in a {Na 4 Cu 4 [(H 2 W 11 O 38 ) (CH 3 COO)(OH) 3 ]} 4 ·88H 2 O (1) and a polyanion Cu-linked {W 11 } chain Na 6 Cu 2 [(H 2 W 11 O 38 )(CH 3 COO)(OH)]·26H 2 O (2). Electronically, the redox properties show that both compounds 1 and 2 undergo irreversible reductions resulting in the demetalation of the compounds, whilst the magnetic behavior of 1 and 2 shows a weak antiferromagnetic and a stronger ferromagnetic coupling, respectively.

chemical communications

Encapsulation of a {Cu16} cluster containing four [Cu4O4] cubanes within an isopolyoxometalate {W44} cluster