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Appel reaction conditions have been harnessed to affect a mild biosynthetically inspired dehydration of endoperoxides to deliver multi-substituted electron rich furans. Unlike traditional dehydrative procedures, this method is metal and acid free, and can be achieved under redox neutral conditions. It is general for a range of aryl and alkyl substituted endoperoxides, and is functional group tolerant. Furthermore, this procedure has been used to deliver an effective total synthesis of the furan fatty acid (FFA) F 5 .

A biosynthetically inspired route to substituted furans using the Appel reaction: total synthesis of the furan fatty acid F5

A biosynthetically inspired route to substituted furans using the Appel reaction: total synthesis of the furan fatty acid F₅