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The simple direct synthesis of Cu(ii) and Ag(i) salts and thiobenzoic acid under ambient conditions allows the preparation of two bidimensional coordination polymers [M(TB)] (TB = thiobenzoate; M = Cu (1) or Ag (2)). Their electrical and luminescent properties show that these are multifunctional materials. Interestingly 1 and 2 undergo a reversible solubilization process. This unusual feature and their simple preparation allow us to prepare a crystalline and free-standing thin-film of 2, using an interfacial procedure, which shows a remarkable thermochromic luminescence.This work was supported by MICINN (MAT2013-46753-C2-1-P and reference CTQ2013-48635-C2-1-P) and Generalitat Valenciana (projects PrometeoII/2014/076 and ISIC).Peer Reviewe

A crystalline and free-standing silver thiocarboxylate thin-film showing high green to yellow luminescence