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Heterobimetallic Pd-K carbenes featuring Pd-C carbene -K moieties were synthesized via an unprecedented sequential substitution/reduction reaction from a radical precursor, [{PC˙(sp 2 )P}  t Bu PdI] ([PC(sp 2 )P]  t Bu = bis[2-(di-iso-propylphosphino)-4- tert -butylphenyl]methylene). Polymeric structures were observed in the solid state for the heterobimetallic compounds that can be interrupted in the presence of a donor solvent.

Heterobimetallic Pd–K carbene complexes via one-electron reductions of palladium radical carbenes