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A systematic study on the microwave-assisted thermolysis of the single source precursor (Et 2 Sb) 2 Te (1) in different asymmetric 1-alkyl-3-methylimidazolium- and symmetric 1,3-dialkylimidazolium-based ionic liquids (ILs) reveals the distinctive role of both the anion and the cation in tuning the morphology and microstructure of the resulting Sb 2 Te 3 nanoparticles as evidenced by X-ray diffraction (XRD), scanning electron microscopy (SEM), energy dispersive X-ray analysis (EDX), and X-ray photoelectron spectroscopy (XPS). A comparison of the electrical and thermal conductivities as well as the Seebeck coefficient of the Sb 2 Te 3 nanoparticles obtained from different ILs reveals the strong influence of the specific IL, from which C 4 mimI was identified as the best solvent, on the thermoelectric properties of as-prepared nanosized Sb 2 Te 3 . This work provides design guidelines for ILs, which allow the synthesis of nanostructured thermoelectrics with improved performances.

Improving the zT value of thermoelectrics by nanostructuring: tuning the nanoparticle morphology of Sb2Te3by using ionic liquids

Improving the zT value of thermoelectrics by nanostructuring: tuning the nanoparticle morphology of Sb₂Te₃by using ionic liquids