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The synthesis of a η 5 -coordinated LiCp complex by simple addition of a Li-salt in benzene is presented. A strongly zwitterionic fulvalene serves as the Cp-precursor. Evidence for the coordination of Li + was obtained by the characterisitic 7 Li NMR chemical shifts, variable temperature experiments in solution and by X-ray structure analysis in the solid state.

Synthesis of a lithium–cyclopentadienide complex by addition of LiNTf2 to a zwitterionic fulvalene

Synthesis of a lithium–cyclopentadienide complex by addition of LiNTf₂ to a zwitterionic fulvalene