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R/X exchange reactions in cis-[M(R) 2 {P(X)(NMeCH 2 ) 2 } 2 ] (M = Pd, Pt; R = aryl, alkyl; X = Cl, Br) were achieved for the first time to give cis-[M(X) 2 {P(R)(NMeCH 2 ) 2 } 2 ]. DFT calculations suggested that the exchange reaction proceeds via a phosphenium intermediate.

R/X exchange reactions in cis-[M(R)2{P(X)(NMeCH2)2}2] (M = Pd, Pt), via a phosphenium intermediate

R/X exchange reactions in cis-[M(R)₂{P(X)(NMeCH₂)₂}₂] (M = Pd, Pt), via a phosphenium intermediate