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A unique, slightly distorted square prismatic, box-like coordination cage of type [Cu 6 Dy 8 L 8 (MeOH) 8 (H 2 O) 6 ](NO 3 ) 12 · χ solvent has been synthesized  via  the supramolecular assembly between a non-centrosymmetric Dy( iii ) metalloligand and Cu( ii ) nitrate.

Self-assembly of a unique 3d/4f heterometallic square prismatic box-like coordination cage