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The reaction of the methylidyne complex [W(CH)Br(CO) 2 (dcpe)] (dcpe = 1,2-bis(dicyclohexylphosphino)ethane) with  t BuLi affords the intermediate anionic neopentylidyne complex Li[W(C t Bu)(CO) 2 (dcpe)] which acts as a metal-based nucleophile towards  t BuCl,  t BuBr, Ph 2 E 2  (E = S, Se, Te) and ClSnMe 3  to afford the new carbyne complexes [W(C t Bu)(X)(CO) 2 (dcpe)] (X = Cl, Br, EPh, SnMe 3 ).

An anionic nucleophilic d4 carbyne complex

An anionic nucleophilic d⁴ carbyne complex