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The phase changes that occur during lithium extraction from LiCoPO 4 in lithium half-cells were studied using synchrotron X-ray diffraction. The existence of two two-phase regions with an intermediate phase present was observed. Significant variations in the composition of the phases of nominal stoichiometry LiCoPO 4 , Li 2/3 CoPO 4 and CoPO 4 resulted in unit cell volume variations. On current pulsing, lattice parameter shifts and phase recovery were directly observed.

In situ phase behaviour of a high capacity LiCoPO4 electrode during constant or pulsed charge of a lithium cell

In situ phase behaviour of a high capacity LiCoPO₄ electrode during constant or pulsed charge of a lithium cell