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The reaction of a variety of N 6 -aryl 2'-deoxyadenosine and adenosine derivatives with PhI(OAc) 2 in 1,1,1,3,3,3-hexafluoro-2-propanol provides a facile access to benzimidazopurine nucleoside analogues by metal-free C-N bond formation with a purinyl nitrogen atom. These reactions likely proceed via radical-cation/radical processes as indicated by radical inhibition experiments.

Benzimidazopurine nucleosides from N6-aryl adenosine derivatives by PhI(OAc)2-mediated C–N bond formation, no metal needed

Benzimidazopurine nucleosides from N⁶-aryl adenosine derivatives by PhI(OAc)₂-mediated C–N bond formation, no metal needed