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The Ritter-type amination of a tertiary C-H bond using iodic acid (HIO 3 ) as an oxidant, in the presence of N-hydroxyphthalimide (NHPI) is reported. This operationally simple method is conducted under metal-free conditions, is scalable, and efficiently provides valuable α-tertiary amine derivatives.

Ritter-type amination of C–H bonds at tertiary carbon centers using iodic acid as an oxidant