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RbCl and CsCl react with BrF 3 yielding the corresponding decafluoridotribromates(iii), MBr 3 F 10 (M = Rb, Cs), which were structurally characterized for the first time. The Br 3 F 10  - anion is surprisingly not linear but contains a μ 3 -bridging fluorine atom and seems to be the first example of μ 3 -F bridging of Br atoms. The compounds are highly reactive and cannot be handled in glassware. As for the tetrafluoridobromates themselves, they are powerful oxidizers and thus suitable for the dry-chemical recycling of precious metals and additionally feature a significantly higher BrF 3 content.

chemical communications

Br2F7− and Br3F10−: peculiar anions showing μ2- and μ3-bridging F-atoms