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Interesting reactivity was observed in reactions of SO 2 with [Zn(Cp*) 2 ] and [(Cp*)Zn I -Zn I (Cp*)]. These reactions proceeded with insertion of SO 2 into the Zn-C bonds. Spectacularly, the lability of the C-S bond in the O 2 SCp* ligands led to the thermal decomposition of [Zn(O 2 SCp*) 2 (tmeda)] to afford [Zn 2 (μ-SO 3 )(μ-S 2 O 4 )(tmeda) 2 ].

Activation of SO2 by [Zn(Cp*)2] and [(Cp*)ZnI–ZnI(Cp*)]

Activation of SO₂ by [Zn(Cp)₂] and [(Cp)Zn^I–Zn^I(Cp*)]