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Low temperature 1 H- and 19 F-DOSY have been used for analyzing reactive intermediates in glycosylation reactions, where a glycosyl trichloroacetimidate donor has been activated using different catalysts. The DOSY protocols have been optimized for low temperature experiments and provided new insight into acid catalyzed glycosylation chemistry. From the study a new glycosylation intermediate was characterized.

chemical communications

Glycosylation intermediates studied using low temperature<sup>1</sup>H- and<sup>19</sup>F-DOSY NMR: new insight into the activation of trichloroacetimidates

Glycosylation intermediates studied using low temperature1H- and19F-DOSY NMR: new insight into the activation of trichloroacetimidates

Glycosylation intermediates studied using low temperature¹H- and¹⁹F-DOSY NMR: new insight into the activation of trichloroacetimidates