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The economic amide base lithium dicyclohexylamide (Cy 2 NLi) allows fast and convenient (40 s, 0 °C) in situ trapping flow metalations of a broad range of functionalized arenes, heteroarenes and acrylate derivatives in the presence of various metal salts (ZnCl 2 ·2LiCl, MgCl 2 , LaCl 3 ·2LiCl). The resulting Zn-, Mg- or La-organometallic intermediates are trapped with various electrophiles in high yields. These flow metalations are easily scaled-up without further optimization.

chemical science

Practical and economic lithiations of functionalized arenes and heteroarenes using Cy<sub>2</sub>NLi in the presence of Mg, Zn or La halides in a continuous flow

Practical and economic lithiations of functionalized arenes and heteroarenes using Cy2NLi in the presence of Mg, Zn or La halides in a continuous flow

Practical and economic lithiations of functionalized arenes and heteroarenes using Cy₂NLi in the presence of Mg, Zn or La halides in a continuous flow