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Reductive deprotection of the trityl group from [Th(ECPh 3 )(NR 2 ) 3 ] (E = O, S), by reaction with KC 8 , in the presence of 18-crown-6, affords the thorium oxo complex, [K(18-crown-6)][Th(O)(NR 2 ) 3 ], and the thorium sulphide complex, [K(18-crown-6)][Th(S)(NR 2 ) 3 ], respectively.

Thorium–ligand multiple bonds via reductive deprotection of a trityl group