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Alkali lignin has been accumulated as a by-product mixed with barium salts during the hydrothermal treatment of rye straw with Ba(OH)2. Direct heat treatment followed by acid washing of such mineralized lignin were performed in order to obtain a porous material that was further exploited for the synthesis of a carbonaceous supported FeNi nanoparticle composite as active catalysts for continuous hydrogenation

Valorization of lignin waste from hydrothermal treatment of biomass: towards porous carbonaceous composites for continuous hydrogenation