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An intermetallic NiSix coating layer was introduced on the Si surface by sputtering Ni onto Si, followed by heat-treatment. The resulting chemically bonded NiSix layer, unlike physically coated layers that typically can crack and detach from Si surfaces upon repeated cycling, remains connected with the bulk Si as a skin-like protective surface.

Improving cyclic performance of Si anode for lithium-ion batteries by forming an intermetallic skin